Chemical Engineering • 7th SemesterCore / Standard CurriculumChange Track

Chemical Engineering — 7th Semester Syllabus

Chemical Engineering

Credits Allocation Table (L-T-P Structure)

Course TitleCodeLTPCredits
Mass Transfer Operations1147013003
Program Elective II1147XX3003
Mass Transfer Operations Lab114701P0021
Summer Internship II114706008 Weeks8
Project-I1147070006
NPTEL Course II1147080002
TOTAL----23

Mass Transfer Operations

114701
Theory Course • 6 Units
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Unit 1: Diffusion: Fundamentals and Applications in Mass Transfer

  • Introduction To Diffusion: Concept
  • Significance
  • And Role Of Diffusion In Mass Transfer And Separation Processes
  • Types Of Diffusion: Molecular Diffusion
  • Eddy Diffusion
  • And Knudsen Diffusion Mechanisms And Comparative Analysis
  • Fundamental Principles Of Diffusion: Fick's First Law Of Diffusion: Diffusional Flux
  • Concentration Gradient
  • Assumptions
  • Derivation
  • And Limitations
  • Fick's Second Law Of Diffusion: Unsteady-state Diffusion
  • Mathematical Formulation
  • And Solution For Simple Boundary Conditions
  • Steady-State Molecular Diffusion In Gases And Liquids: Diffusion Of A Gas A Through A Stagnant Gas B
  • Equimolar Counter Diffusion
  • Diffusion In Liquids Binary Diffusivity
  • Interdiffusion
  • And Factors Influencing Diffusivity (Temperature, Pressure, Molecular Weight, And Medium)
  • Numerical Problems: Application Of Fick's Laws To Steady And Unsteady Diffusion In Gases And Liquids

Unit 2: Distillation

  • Introduction: Definition And Importance Of Distillation In Separation Processes
  • Concept And Basic Principles Of Distillation
  • Vapour-Liquid Equilibrium (VLE): Phase Behaviour And Boiling Point Diagram
  • Equilibrium Diagram And Relative Volatility
  • Effect Of Pressure On VLEP-x-y Diagrams
  • Ideal Solutions: Raoult's Law
  • Non-ideal Solutions: Henry's Law And Deviations From Ideality
  • Distillation Methods: Distillation Without Fractionation
  • Flash Vaporization: Principle
  • Operation
  • And Material Balance
  • Simple Distillation: Principle
  • Operation
  • Material Balance
  • And Rayleigh's Equation
  • Steam Distillation: Principle
  • Operation
  • And Material Balance
  • Distillation With Fractionation: Principle Of Fractionation And Types Of Refluxes (Total, Minimum, And Optimum)
  • Material Balance: Overall And Component Material Balance For Distillation Columns
  • McCabe-Thiele Method: Determination Of Theoretical Stages/Plates: Construction Of Operating Lines For Rectifying And Stripping Sections
  • Feed Line (q-line): Feed Quality
  • Equation
  • And Effect On Slope
  • Numerical Problems: Determination Of Number Of Theoretical Plates By McCabe-Thiele Method
  • Types Of Fractionating Columns: Plate Columns: Bubble-cap
  • Sieve
  • And Valve Plates
  • Packed Columns: Random And Structured Packings
  • Column Internals: Weirs And Downcomers

Unit 3: Gas Absorption

  • Introduction: Definition
  • Concept
  • And Basic Principles Of Gas Absorption
  • Importance Of Gas-liquid Mass Transfer Operations In Process Industries
  • Distinction Between Absorption And Adsorption Phenomena With Suitable Industrial Examples
  • Applications Of Absorption In Chemical
  • Petrochemical
  • And Environmental Engineering (e.g., Removal Of CO2, SO2, And NH3 From Gas Streams)
  • Absorption Equilibrium: Concept Of Solubility Of Gases In Liquids And Equilibrium Relations Between Gas And Liquid Phases
  • Use Of Henry's Law And Raoult's Law In Describing Gas Absorption Equilibrium
  • Influence Of Temperature
  • Pressure
  • And Solute Concentration On Solubility
  • Application Of The Phase Rule To Gas-liquid Systems
  • Criteria For Selection Of Solvents For Specific Absorption Duties Based On Solubility
  • Selectivity
  • Volatility
  • Chemical Stability
  • Viscosity
  • Cost
  • And Ease Of Regeneration
  • Gas Absorption Equipment: Types
  • Principles
  • And Design Fundamentals
  • Major Gas Absorption Equipment Used In Industry
  • Including Packed Columns
  • Plate Columns
  • And Mechanically Agitated Vessels
  • Packed Columns: Constructional Features
  • Operating Principles
  • And Design Fundamentals Of Packed Towers
  • Characteristics And Performance Parameters Of Structured Packings (Metallic Or Plastic Corrugated Sheets, Wire Mesh) And Random Packings (Raschig Rings, Pall Rings, Berl And Intalox Saddles)
  • Packing Characteristics
  • Mass Transfer Area
  • And Pressure Drop Through Packed Beds
  • Hydrodynamics In Packed Columns
  • Including Liquid Holdup
  • Channeling
  • Flooding
  • And Loading Behavior
  • Definition And Significance Of Height Equivalent To A Theoretical Plate (HETP) And Its Correlation With Column Performance
  • Numerical Problems Based On Design And Performance Of Packed Columns
  • Mechanically Agitated Vessels: Principle
  • Design Features
  • Working
  • And Application In Gas Absorption Operations Where High Gas-liquid Contact Efficiency Is Required
  • Material Balance And Power Consumption
  • Venturi Scrubber: Principle Of Operation
  • Design Features
  • Hydrodynamic Behavior
  • And Mass Transfer Mechanism
  • Advantages
  • Limitations
  • And Industrial Applications In Removing Fine Particulate Matter And Soluble Gases From Gas Streams

Unit 4: Liquid-Liquid Extraction

  • Introduction: Definition
  • Concept
  • And Basic Principles Of Liquid-liquid Extraction As A Mass Transfer Operation
  • Importance Of Extraction In Separating Components From Liquid Mixtures Where Distillation Is Ineffective Due To Close Boiling Points
  • Heat Sensitivity
  • Or Azeotrope Formation
  • Comparison Between Extraction And Distillation Based On Driving Force
  • Equipment
  • And Industrial Applications
  • Liquid Equilibria: Equilibrium Distribution Of Solute Between Two Immiscible Liquid Phases And Derivation Of The Distribution Law
  • Representation Of Equilibrium Data Using Distribution Coefficient And Its Dependence On Temperature And Solute Concentration
  • Graphical Representation Of Equilibrium Using Equilateral Triangular Coordinates And Ternary Phase Diagrams For Systems Containing One Pair Partially Miscible And Two Pairs Partially Miscible
  • Interpretation Of Tie Lines
  • Plait Point
  • And Binodal Curve In Ternary Diagrams
  • Determination Of The Number Of Theoretical Stages In Extraction Using Graphical Methods
  • Numerical Problems Based On Distribution Coefficient And Extraction Efficiency
  • Choice Of Solvent: Selection Criteria For Solvents Used In Extraction
  • Including High Selectivity For Solute
  • Low Miscibility With The Feed Liquid
  • Chemical Stability
  • Low Viscosity
  • Ease Of Regeneration
  • Non-toxicity
  • Availability
  • And Cost-effectiveness
  • Solvent Recovery And Economic Considerations In Extraction Processes
  • Extraction Equipment: Various Types Of Liquid-liquid Extraction Equipment Used In Industrial Practice
  • Emphasizing Their Principle
  • Construction
  • Working
  • And Application
  • Mixer-Settler Assemblies: Design And Operation Of Mixer-settler Units
  • Principle Of Dispersion And Phase Separation
  • Application In Batch And Continuous Extraction Processes
  • Static Columns: Design And Operation Of Spray Columns And Sieve Plate Columns
  • Flow Pattern
  • Contact Efficiency
  • Residence Time
  • And Operating Limitations
  • Mechanically Agitated Columns: Working Principles And Design Features Of Rotating Disc Contactors (RDC) And Pulse Columns
  • Effect Of Agitation Speed
  • Droplet Size
  • And Column Dimensions On Mass Transfer Rate And Extraction Efficiency
  • Centrifugal Contactors: Principle And Design Aspects Of Centrifugal Extractors
  • Advantages Such As High Mass Transfer Efficiency
  • Compact Design
  • And Short Residence Time
  • Industrial Applications In Solvent Recovery
  • Metal Extraction
  • And Pharmaceutical Industries

Unit 5: Crystallization

  • Introduction: Definition
  • Importance
  • And Fundamental Concept Of Crystallization As A Separation And Purification Process
  • Applications Of Crystallization In Chemical
  • Pharmaceutical
  • And Food Industries
  • Crystal Formation As A Simultaneous Process Of Mass Transfer And Thermodynamic Equilibrium
  • Mechanism Of Crystallization: Concepts Of Saturation
  • Supersaturation
  • And Nucleation
  • Explanation Of Mier's Theory Of Supersaturation And Its Role In Controlling Crystal Size And Purity
  • Distinction Between Primary And Secondary Nucleation And Between Crystal Growth And Nucleation Kinetics
  • Factors Affecting Crystal Formation Such As Temperature
  • Concentration
  • Agitation
  • And Impurities
  • Crystallization Equipment: Principle
  • Construction
  • Operation And Performance Of Major Crystallizers Used In Industry
  • Detailed Design And Working Of Agitated Tank Crystallizer And Swenson-Walker Crystallizer
  • Process Parameters Influencing Product Yield And Quality

Unit 6: Drying

  • Introduction: Definition
  • Significance
  • And Basic Principles Of Drying As A Mass Transfer Operation
  • Importance Of Drying In Process Industries For Solid-liquid Separation
  • Moisture Removal
  • And Product Preservation
  • Modes Of Drying: Constant-rate And Falling-rate Periods
  • Drying Equilibrium: Concept Of Drying Equilibrium And Representation Of Moisture Content On Dry Basis And Wet Basis
  • Relationship Between Relative Humidity And Moisture Content Of Solids
  • Explanation Of Equilibrium Moisture Content
  • Free Moisture
  • Bound And Unbound Water
  • Hysteresis
  • And The Effect Of Soluble Solids On Drying Characteristics
  • Development And Interpretation Of Drying Rate Curves
  • Numerical Problems Based On Drying Equilibrium And Rate Calculations
  • Drying Equipment: Classification Of Dryers Into Batch And Continuous Types
  • Principles
  • Construction
  • Working
  • And Applications Of Common Industrial Dryers Including Tray Dryer
  • Rotary Dryer
  • Drum Dryer
  • Spray Dryer
  • And Fluidized Bed Dryer
  • Comparative Analysis Of These Dryers Based On Heat And Mass Transfer Rates
  • Energy Efficiency
  • And Suitability For Different Materials
  • Process Optimization
  • Drying Kinetics
  • And Scale-up Considerations

Program Elective II

1147XX
Theory Course • Course Details
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Available Elective Tracks & Options (4):

Program Elective II: Bioprocess Engineering

114702

Unit 1

Introduction To Bioprocesses • Historical Development Of Bioprocess Technology • An Overview Of Traditional And Modern Applications Of Biotechnology Industry • Outline Of An Integrated Bioprocess And The Various (upstream And Downstream) Unit Operations Involved In Bioprocess • Generalized Process Flow Sheets

Unit 2

Fermentation Process-I: General Requirements Of Fermentation Processes • Basic Design And Construction Of Fermenter And Ancillaries • Main Parameters To Be Monitored And Controlled In Fermentation Process • Fermentation Process-II: An Overview Of Aerobic And Anaerobic Fermentation Processes And Their Application In The Biotechnology Industry • Solid-substrate • Slurry Fermentation And Its Applications • Whole Cell Immobilization • Behaviour Of Microbes In Different Reactors (Air Lift, Fluidized, Batch, Continuous Fed Batch Condition)

Unit 3

Media Design: Medium Requirements For Fermentation Process • Carbon • Nitrogen • Minerals • Vitamins And Other Complex Nutrients • Oxygen Requirements • Medium Formulation For Optimal Growth And Product Formation • Examples Of Simple And Complex Media • Design And Usage Of Various Commercial Media For Industrial Fermentations • Sterilization: Thermal Death Kinetics Of Microorganisms • Batch And Continuous Heat • Sterilization Of Liquid Media • Filter Sterilization Of Liquid Media • Air • Design Of Sterilization Equipment

Unit 4

Kinetics Of Microbial Growth And Product Formation: Phases Of Cell Growth In Batch Cultures • Simple Unstructured Kinetic Models For Microbial Growth • Monod Model • Growth Of Filamentous Organisms • Growth Associated (Primary) And Nongrowth Associated (Secondary) Product Formation Kinetics • Leudeking-Piret Models • Substrate And Product Inhibition On Cell Growth And Product Formation • Introduction To Structured Models For Growth And Product Formation

Unit 5

Metabolic Stoichiometry: Stoichiometry Of Cell Growth And Product Formation • Elemental Balances • Degrees Of Reduction Of Substrate And Biomass • Available Electron Balances • Yield Coefficients Of Biomass And Product Formation • Maintenance Coefficients

Unit 6

Energetics: Energetic Analysis Of Microbial Growth And Product Formation • Oxygen Consumption And Heat Evolution In Aerobic Cultures Thermodynamic Efficiency Of Growth

Program Elective II: Disaster Management

114703

Unit 1: Fundamentals of Disaster Management

Definitions And Concepts Of Hazard • Vulnerability • Risk • Resilience • Concept Of Disaster Management Cycle • Introduction To Various Hazards Both Natural And Man-Made Hazards- Earthquakes • Cyclones • Droughts • Floods • Volcanoes • Coastal Hazards • Landslides • Forest Fires • Industrial Accidents • Biological Disasters • Etc. • Climate Change • Global Warming

Unit 2: Disaster Management in India

Hazard And Vulnerability Profile Of India • Disaster Management Act 2005 • National Disaster Mitigation And Management Guideline On -National Policy On Disaster Management 2009 • NDMA Guidelines On Cyclones Specifically • Besides Earthquakes • Floods • Urban Floods • Information Systems • Communication Systems Etc. • Introduction To State Disaster Management Authorities

Unit 3: Hazard Analysis

Estimation Of Potential Causes • Characteristics And Impact Of Hazards • Geological/Processes Leading To Natural Hazards • Multi-Hazard Assessment • Short Term And Long Term Prediction • Early Warning System For Different Hazards • Risk Analysis For Individuals • Communities Etc. • Role Of Remote Sensing & GIS In Disaster Management And Its Applications • Case Studies • Sudden Explosion Of Cylinder • Bulk Chemical Storage Fire

Unit 4: Disaster Risk Reduction (DRR)

Assessing Vulnerabilities • Risk Assessment • Preparation Of Exposure And Risk Database • Prevention And Mitigation Strategies For DRR • Framework Of Disaster Risk Reduction • Capacity Building Measures • Community Participation • Contemporary Studies And Work Towards Disaster Risk Reduction • Disaster Risk Reduction Plan

Unit 5: Response & Recovery Operation I

Role Of NDRF • Training Of Personnel • Equipment Necessary • Public Awareness Creation • Mass Casualty Management • Agencies Involved In Mass Casualty Management • Qualification And Duties Of Professionals • Response Policy

Unit 6: Response & Recovery Operation II

Case Studies: Case Study: Recover & Rehabilitation After Bhopal Gas Tragedy • The Indian Ocean Tsunami 2004 • The 2013 IOCL Hazira Fire Accident

Program Elective II: Membrane Technology

114704

Unit 1: Introduction to Membrane Technology

History And Evolution Of Membrane Technology • Classification Of Membranes • Basic Principles Of Membrane Separation • Transport Mechanisms: Diffusion • Osmosis • Filtration • Dead End And Crossflow Membrane Process

Unit 2: Membrane Materials and Fabrication

Types Of Membrane Materials (Polymeric, Ceramic, Metallic, Composite) • Fabrication Techniques (Phase Inversion, Electrospinning, Sintering) • Membrane Structure: Symmetric Vs. Asymmetric • Characterization Methods (SEM, AFM, Porometry, Spectroscopy)

Unit 3: Membrane Processes and Membrane Modules

Overview Of Membrane Separation Processes: A) Microfiltration (MF) • B) Ultrafiltration (UF) • C) Nanofiltration (NF) • D) Reverse Osmosis (RO) • E) Forward Osmosis (FO) • F) Gas Separation • G) Pervaporation • H) Electrodialysis • Membrane Modules: A) Plate-and-frame • B) Spiral-wound • C) Hollow Fiber • D) Tabular

Unit 4: Applications of Membrane Technology

Membrane Bioreactor For Wastewater Treatment • Desalination By Membrane Technology • Separation Of Azeotropic Mixture Using Pervaporation Membrane Process • Food And Beverage Industry (e.g., Dairy, Juice Concentration) • Pharmaceutical And Biotechnology Applications • Energy Sectors (e.g., Hydrogen Production, Carbon Capture) • Emerging Areas: Membranes In Batteries And Fuel Cells

Unit 5: Challenges, Innovations and Future Trends I

Membrane Fouling And Cleaning Strategies • Economic Considerations (Cost Analysis, Lifecycle Assessment)

Unit 6: Challenges, Innovations and Future Trends II

Advances In Membrane Materials (Graphene, MOFs, Aquaporin-based Membranes) • Sustainability And Environmental Impacts • Future Directions: Smart Membranes • Bioinspired Membranes

Program Elective II: Renewable Energy Technology

114705

Unit 1: Introduction to Renewable Energy

Global And National Energy Scenarios • Types Of Renewable Energy Sources • Need For Renewable Energy: Environmental And Economic Perspectives • Energy Units And Conversions • Energy Balance And Efficiency Calculations • Conventional • Non-conventional • Renewable • Non-renewable Sources Of Energy: Prospects • Perspectives • & Advantages • Types Of Energy Storage: Thermal • Electrochemical (Batteries) • Mechanical (Flywheels) • Chemical (Hydrogen)

Unit 2: Solar Energy

Solar Thermal Systems: Solar Collectors (Flat Plate, Evacuated Tube, Concentrating) • Heat Transfer Fluids And Materials • Solar Water Heating Systems • Photovoltaic (PV) Systems: Working Principle And Components • Efficiency And Performance Analysis • PV Cell Materials (Silicon-based, Thin-film, Emerging Technologies) • Performance Analysis Of Liquid Flat Plate Collectors And Solar Air Heaters • Chemical Applications: Solar-assisted Chemical Reactors • Solar Hydrogen Production (Photocatalysis, Thermolysis)

Unit 3: Hydrogen and Fuel Cells

Hydrogen As An Energy Carrier • Production Methods: Steam Methane Reforming (SMR) • Electrolysis (Alkaline, PEM) • Thermochemical Water Splitting • Hydrogen Storage And Transport • Fuel Cell Types: Proton Exchange Membrane Fuel Cell (PEMFC) • Solid Oxide Fuel Cell (SOFC) • Direct Methanol Fuel Cell (DMFC)

Unit 4: Wind Energy

Wind Energy: Wind Turbine Types • Aerodynamics • Wind Farm Siting And Design • Power Generation And Control Systems

Unit 5: Hydropower Energy

Hydropower: Principles Of Hydropower • Small-scale Hydro Systems • Environmental Impacts And Mitigation

Unit 6: Geothermal and Ocean Energy

Geothermal Resources And Extraction Technologies • Binary Cycle And Flash Steam Plants • Ocean Energy: Tidal And Wave Energy Conversion • Ocean Thermal Energy Conversion (OTEC)

NPTEL Course II

114708
Theory Course • Course Details
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Mass Transfer Operations Lab

114701P
Laboratory Subject • 1 Units
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List of Experiments:

  • 1. Determination Of The Diffusion Coefficient Of A Given Gas Or Vapor In Air Using A Diffusion Cell
  • 2. Determination Of The Diffusivity Of A Solute In A Liquid Medium Using A Diffusion Cell
  • 3. Verification Of Rayleigh's Equation In Simple Distillations
  • 4. Determination Of Vapour-Liquid Equilibrium (VLE) Data For A Binary Mixture
  • 5. Performance Evaluation Of A Fractional Distillation Column For Separation Of Binary Mixtures
  • 6. Performance Evaluation Of A Packed Column For Gas Absorption
  • 7. Determination Of Distribution Coefficient Of A Solute From A Liquid Mixture Using A Suitable Solvent For Liquid-Liquid Extraction In A Mixer Settler Unit
  • 8. Determination Of The Crystal Yield And Crystal Size Distribution By Performing Batch Crystallization Of A Solution In A Batch Crystallizer
  • 9. Determination Of The Drying Rate And Equilibrium Moisture Content Using A Tray Dryer
  • 10. Evaluation Of Hydrodynamics In A Packed Column
  • 11. Determination Of The Percentage Recovery Of An Essential Oil By Using Steam Distillation Apparatus
  • 12. Determination Of Height Equivalent To Theoretical Plates (HETP) In A Packed Distillation Column
  • 13. Determination Of Drying Rate Of A Wet Solid Using A Fluidized Bed Dryer
  • 14. Performance Analysis Of A Rotary Dryer To Investigate The Drying Efficiency And Residence Time Of Solids In A Rotary Dryer
  • 15. Analysis Of The Role Of An Entrainer In Breaking The Azeotrope By Performing Azeotropic Distillation

Prescribed Experiments

  1. List of Experiments: 1. Determination Of The Diffusion Coefficient Of A Given Gas Or Vapor In Air Using A Diffusion Cell 2. Determination Of The Diffusivity Of A Solute In A Liquid Medium Using A Diffusion Cell 3. Verification Of Rayleigh's Equation In Simple Distillations 4. Determination Of Vapour-Liquid Equilibrium (VLE) Data For A Binary Mixture 5. Performance Evaluation Of A Fractional Distillation Column For Separation Of Binary Mixtures 6. Performance Evaluation Of A Packed Column For Gas Absorption 7. Determination Of Distribution Coefficient Of A Solute From A Liquid Mixture Using A Suitable Solvent For Liquid-Liquid Extraction In A Mixer Settler Unit 8. Determination Of The Crystal Yield And Crystal Size Distribution By Performing Batch Crystallization Of A Solution In A Batch Crystallizer 9. Determination Of The Drying Rate And Equilibrium Moisture Content Using A Tray Dryer 10. Evaluation Of Hydrodynamics In A Packed Column 11. Determination Of The Percentage Recovery Of An Essential Oil By Using Steam Distillation Apparatus 12. Determination Of Height Equivalent To Theoretical Plates (HETP) In A Packed Distillation Column 13. Determination Of Drying Rate Of A Wet Solid Using A Fluidized Bed Dryer 14. Performance Analysis Of A Rotary Dryer To Investigate The Drying Efficiency And Residence Time Of Solids In A Rotary Dryer 15. Analysis Of The Role Of An Entrainer In Breaking The Azeotrope By Performing Azeotropic Distillation
  2. 1. Determination Of The Diffusion Coefficient Of A Given Gas Or Vapor In Air Using A Diffusion Cell
  3. 2. Determination Of The Diffusivity Of A Solute In A Liquid Medium Using A Diffusion Cell
  4. 3. Verification Of Rayleigh's Equation In Simple Distillations
  5. 4. Determination Of Vapour-Liquid Equilibrium (VLE) Data For A Binary Mixture
  6. 5. Performance Evaluation Of A Fractional Distillation Column For Separation Of Binary Mixtures
  7. 6. Performance Evaluation Of A Packed Column For Gas Absorption
  8. 7. Determination Of Distribution Coefficient Of A Solute From A Liquid Mixture Using A Suitable Solvent For Liquid-Liquid Extraction In A Mixer Settler Unit
  9. 8. Determination Of The Crystal Yield And Crystal Size Distribution By Performing Batch Crystallization Of A Solution In A Batch Crystallizer
  10. 9. Determination Of The Drying Rate And Equilibrium Moisture Content Using A Tray Dryer
  11. 10. Evaluation Of Hydrodynamics In A Packed Column
  12. 11. Determination Of The Percentage Recovery Of An Essential Oil By Using Steam Distillation Apparatus
  13. 12. Determination Of Height Equivalent To Theoretical Plates (HETP) In A Packed Distillation Column
  14. 13. Determination Of Drying Rate Of A Wet Solid Using A Fluidized Bed Dryer
  15. 14. Performance Analysis Of A Rotary Dryer To Investigate The Drying Efficiency And Residence Time Of Solids In A Rotary Dryer
  16. 15. Analysis Of The Role Of An Entrainer In Breaking The Azeotrope By Performing Azeotropic Distillation

Summer Internship II

114706
Laboratory Subject • Course Details
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Project-I

114707
Laboratory Subject • Course Details
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